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Column | Rtx-PCB, 60 m, 0.25 mm ID, 0.25 µm (cat.# 13226) |
---|---|
Standard/Sample | Aroclor 1242 (cat.# 32009) |
Aroclor 1254 (cat.# 32011) | |
Aroclor 1262 (cat.# 32409) | |
Conc.: | 333 ppm each |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.75 min) |
Liner: | Splitless taper (4 mm) w/wool (cat.# 22405) |
Inj. Temp.: | 280 °C |
Oven | |
Oven Temp.: | 100 °C (hold 1 min) to 200 °C at 30 °C/min to 320 °C at 2 °C/min (hold 1 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.1 mL/min |
Detector | MS |
---|---|
Mode: | Scan |
Transfer Line Temp.: | 280 °C |
Ionization Mode: | EI |
Scan Range: | 50-550 amu |
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