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Peaks | |
---|---|
1. | 2-Fluorophenol |
2. | Phenol-d6- |
3. | 1,4-Dichlorobenzene-d4 |
4. | Nitrobenzene-d5 |
5. | Naphthalene-d8 |
6. | Naphthalene |
7. | 2-Fluorobiphenyl |
8. | Acenaphthylene |
9. | Acenaphthene-d10 |
10. | Acenaphthene |
11. | Fluorene |
12. | 2,4,6-Tribromophenol |
13. | Phenanthrene-d10 |
14. | Phenanthrene |
Peaks | |
---|---|
15. | Anthracene |
16. | Fluoranthene |
17. | Pyrene |
18. | p-Terphenyl-d14 |
19. | Benz[a]anthracene |
20. | Chrysene-d12 |
21. | Chrysene |
22. | Benzo[b]fluoranthene |
23. | Benzo[k]fluoranthene |
24. | Benzo[a]pyrene |
25. | Perylene-d12 |
26. | Indeno[1,2,3-cd]pyrene |
27. | Dibenz[a,h]anthracene |
28. | Benzo[ghi]perylene |
Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) |
---|---|
Standard/Sample | SV Calibration Mix #5 / 610 PAH Mix (cat.# 31011) |
Acid Surrogate Mix (4/89 SOW) (cat.# 31025) | |
B/N Surrogate Mix (4/89 SOW) (cat.# 31024) | |
SV Internal Standard Mix (cat.# 31206) | |
Conc.: | 10 ng/µL each analyte, 40 ng/μL internal standards |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.1 min) |
Liner: | Drilled Uniliner (hole near bottom) (cat.# 20771) |
Inj. Temp.: | 275 °C |
Oven | |
Oven Temp.: | 75 °C (hold 0.5 min) to 245 °C at 25 °C/min to 330 °C at 4 °C/min (hold 1 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.2 mL/min |
Detector | MS |
---|---|
Mode: | Scan |
Transfer Line Temp.: | 280 °C |
Solvent Delay Time: | 2 min |
Tune Type: | DFTPP |
Ionization Mode: | EI |
Scan Range: | 35-550 amu |
Instrument | HP6890 GC & 5973 MSD |
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