Minnesota Dept. of Agriculture List 1 Pesticides on Rxi-1ms

Injection
Column	Rxi-1ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13323)
Standard/Sample	Minnesota Ag List 1 Pesticides Mix A (cat.# 32406)
	Minnesota Ag List 1 Pesticides Mix B (cat.# 32407)
	SV Internal Standard Mix (cat.# 31206)
	B/N Surrogate Mix (4/89 SOW) (cat.# 31024)
	Acid Surrogate Mix (4/89 SOW) (cat.# 31025)
Conc.:	10 µg/mL each analyte (internal standards 25ug/ml)
Inj. Vol.:	1.0 µL split (split ratio 10:1)
Liner:	Drilled Uniliner (hole near bottom) (cat.# 20771)
Inj. Temp.:	250 °C
Oven
Oven Temp.:	70 °C (hold 1 min) to 180 °C at 20 °C/min to 230 °C at 5 °C/min to 325 °C at 40 °C/min (hold 3.5 min)
Carrier Gas	He, constant flow
Flow Rate:	1.2 mL/min

Download PDF