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Semivolatiles on Rxi-5ms by EPA Method 525.2

GC_EV00859
Peaks
1.Isophorone
2.2-Nitro-m-xylene (SS)
3.Naphthalene
4.Dichlorvos (DDVP)
5.Hexachlorocyclopentadiene
6.EPTC
7.Mevinphos
8.Butylate
9.Vernolate
10.Dimethyl phthalate
11.Pebulate
12.Etridiazole
13.2,6-Dinitrotoluene
14.Acenaphthylene
15.Acenaphthene-d10 (IS)
16.Chloroneb
17.Tebuthiuron
18.2,4-Dinitrotoluene
19.Molinate
20.Diethyl phthalate
21.Fluorene
22.Propachlor
23.Ethoprop (ethoprophos)
24.Cycloate
25.Chlorpropham
26.Trifluralin
27.Atraton
28.Hexachlorobenzene
29.Prometon
30.Simazine
31.Atrazine
Peaks
32.Propazine
33.Pentachlorophenol
34.Terbufos
35.Propyzamide
36.Diazinon
37.Phenanthrene-d10 (IS)
38.Phenanthrene
39.Disulfoton
40.Methylparaoxon
41.Anthracene
42.Terbacil
43.Chlorothalonil
44.Metribuzin
45.Simetryn
46.Ametryn
47.Alachlor
48.Prometryn
49.Terbutryn
50.di-n-Butyl phthalate
51.Bromacil
52.Cyanazine (Bladex)
53.Metolachlor
54.Chlorpyrifos
55.Triadimefon
56.DCPA methyl ester (Chlorthal-dimethyl)
57.MGK-264 (isomer A)
58.Diphenamid
59.MGK-264 (isomer B)
60.Merphos
61.Heptachlor epoxide
62.Fluoranthene
Peaks
63.Stirofos
64.Disulfoton sulfone
65.Butachlor
66.Pyrene-d10 (SS)
67.Fenamiphos
68.Pyrene
69.Napropamide (Devrinol)
70.trans-Nonachlor
71.Merphos oxide
72.Tricyclazole (Beam)
73.Carboxin
74.Chlorobenzilate
75.Benzyl butyl phthalate
76.Norflurazon
77.Bis(2-ethylhexyl) adipate
78.Hexazinon (Velpar)
79.Triphenylphosphate (SS)
80.Benz[a]anthracene
81.Chrysene-d12 (IS)
82.Chrysene
83.Bis(2-ethylhexyl) phthalate
84.Fenarimol
85.cis-Permethrin
86.trans-Permethrin
87.Di-n-octyl phthalate
88.Benzo[b]fluoranthene
89.Benzo[k]fluoranthene
90.Benzo[a]pyrene
91.Fluridone (Sonar)
92.Perylene-d12 (SS)
93.Indeno[1,2,3-cd]pyrene
94.Dibenzo[a,h]anthracene
95.Benzo[ghi]perylene
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
Standard/SampleMethod 525.2 semivolatile mix (revised) (cat.# 31899)
Organonitrogen pesticide mix #1 (rev), Method 525.2 (cat.# 33012)
Organochlorine pesticide mix #2 (rev), Method 525.2 (cat.# 33011)
Organophosphorus pesticide mix #1 (rev), Method 525.2 (cat.# 33013)
Method 525.2 nitrogen/phosphorus pesticide mix #2 (cat.# 32423)
Method 525.2 internal standard mix (cat.# 31825)
Method 525.2 surrogate standard mix (cat.# 31826)
Conc.:25 µg/mL for each IS and SS, 10 μg/mL each analyte
Injection
Inj. Vol.:1.0 µL pulsed splitless (hold 0.15 min)
Liner:Drilled Uniliner (hole near bottom) (cat.# 20771)
Inj. Temp.:250 °C
Pulse Pressure:50 psi (344.7kPa)
Pulse Time:0.3 min
Purge Flow:80 mL/min
Oven
Oven Temp.:90 °C (hold 1 min) to 270 °C at 20 °C/min to 315 °C at 6 °C/min
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Solvent Delay Time:3.00 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
InstrumentHP6890 GC & 5973 MSD
NotesGas saver is on at 15 mL/min. (1 minute).
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