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Peaks | |
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1. | 1,4-Dioxane |
2. | N-Nitrosodimethylamine |
3. | Pyridine |
4. | 2-Fluorophenol (SS) |
5. | Phenol-d6 (SS) |
6. | Phenol |
7. | Aniline |
8. | Bis(2-chloroethyl) ether |
9. | 2-Chlorophenol |
10. | 1,3-Dichlorobenzene |
11. | 1,4-Dichlorobenzene-d4 (IS) |
12. | 1,4-Dichlorobenzene |
13. | Benzyl alcohol |
14. | 1,2-Dichlorobenzene |
15. | 2-Methylphenol |
16. | Bis(2-chloroisopropyl) ether |
17. | 4-Methylphenol/3-methylphenol |
18. | N-Nitrosodi-N-propylamine |
19. | Hexachloroethane |
20. | Nitrobenzene-d5 (SS) |
21. | Nitrobenzene |
22. | Isophorone |
23. | 2-Nitrophenol |
24. | 2,4-Dimethylphenol |
25. | Benzoic acid |
26. | Bis(2-chloroethoxy)methane |
27. | 2,4-Dichlorophenol |
28. | 1,2,4-Trichlorobenzene |
29. | Naphthalene-d8 (IS) |
30. | Naphthalene |
31. | 4-Chloroaniline |
Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
---|---|
Standard/Sample | 8270 MegaMix (cat.# 31850) |
Benzoic acid (cat.# 31879) | |
8270 Benzidines mix (cat.# 31852) | |
Acid surrogate mix (4/89 SOW) (cat.# 31025) | |
Revised B/N surrogate mix (cat.# 31887) | |
1,4-Dioxane (cat.# 31853) | |
SV internal standard mix (cat.# 31206) | |
Conc.: | 10 µg/mL (IS 40 μg/mL) |
Injection | |
Inj. Vol.: | 1.0 µL pulsed splitless (hold 0.15 min) |
Liner: | 4 mm drilled Uniliner (hole near bottom) (cat.# 20756) |
Inj. Temp.: | 250 °C |
Pulse Pressure: | 25 psi (172.4kPa) |
Pulse Time: | 0.2 min |
Purge Flow: | 60 mL/min |
Oven | |
Oven Temp.: | 40 °C (hold 1.0 min) to 280 °C at 25 °C/min to 320 °C at 5 °C/min (hold 1 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.2 mL/min |
Detector | MS |
---|---|
Mode: | Scan |
Transfer Line Temp.: | 280 °C |
Ionization Mode: | EI |
Scan Range: | 35-550 amu |
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