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|Column||Rtx-CLPesticides, 30 m, 0.32 mm ID, 0.32 µm (cat.# 11141)|
|Standard/Sample||Aroclor 1221 in hexane diluted to 1,000 ppb|
|decachlorobiphenyl (BZ #209) in acetone diluted to 100 ppb (cat.# 32029)|
|Inj. Vol.:||1.0 µL pulsed splitless (hold 0.3 min)|
|Liner:||Cyclo Double Gooseneck (4mm) (cat.# 20895)|
|Inj. Temp.:||250 °C|
|Pulse Pressure:||30 psi (206.8kPa)|
|Oven Temp.:||120 °C to 200 °C at 45 °C/min to 230 °C at 15 °C/min to 330 °C at 30 °C/min (hold 2 min)|
|Carrier Gas||He, constant linear velocity|
|Linear Velocity:||60 cm/sec @ 120 °C|
|Detector||ECD @ 330 °C|
|Notes||This chromatogram was obtained using an Agilent μ-ECD. To obtain comparable results, you will need to employ a μ-ECD in addition to confirmational dual-columns connected to a 5-meter guard column using a “Y” Press-Tight connector.|