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|Column||Rtx-CLPesticides2, 30 m, 0.32 mm ID, 0.25 µm (cat.# 11324)|
|Standard/Sample||PCB kit #1 diluted to 1,000 ppb in hexane (cat.# 32089)|
|Decachlorobiphenyl (BZ #209) diluted to 100 ppb in acetone (cat.# 32029)|
|Inj. Vol.:||1.0 µL pulsed splitless (hold 0.3 min)|
|Liner:||Cyclo double taper (4 mm) (cat.# 20895)|
|Inj. Temp.:||250 °C|
|Pulse Pressure:||30 psi (206.8kPa)|
|Oven Temp.:||120 °C to 200 °C at 45 °C/min to 230 °C at 15 °C/min to 330 °C at 30 °C/min (hold 2 min)|
|Carrier Gas||He, constant flow|
|Linear Velocity:||60 cm/sec|
|Detector||Micro-ECD @ 330 °C|
|Notes||This chromatogram was obtained using an Agilent micro-ECD. To obtain comparable results, you will need to employ a micro-ECD in addition to confirmational dual columns connected to a 5-meter guard column using a “Y” Press-Tight connector.|