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Peaks | |
---|---|
1. | 3-Nitroaniline |
2. | 2,4-Dinitrophenol |
3. | Pentachlorophenol |
4. | Phenanthrene |
Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
---|---|
Standard/Sample | Phenols/Anilines/Pesticides Test Mix (cat.# 35245) |
Conc.: | 10 ng on-column |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.75 min) |
Liner: | Gooseneck Splitless (4mm) w/Semivolatiles Wool (cat.# 20798-231.1) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 50 °C (hold 3.5 min) to 180 °C at 35 °C/min (hold 3.5 min) to 300 °C at 20 °C/min (hold 0.5 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.2 mL/min |
Detector | FID @ 330 °C |
---|---|
Notes | FID: Hydrogen: 30mL/min. Air: 400mL/min. Nitrogen: 25mL/min. 10ng 2,4-dinitrophenol (DNP) on-column, single gooseneck liner with wool, FID analysis with phenanthrene internal standard. |
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