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Column | Rtx-TNT1, 6 m, 0.53 mm ID, 0.5 µm (cat.# 562719) |
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using IP deactivated guard column 5 m, 0.53 mm ID (cat.# 10045) | |
Standard/Sample | 8095 Calibration mix A (cat.# 31607) |
8095 Calibration mix B (cat.# 31608) | |
Diluent: | Acetonitrile |
Injection | PTV splitless (hold 0.35 min) |
Liner: | PTV on-column liner (cat.# 24976) |
Inlet Temp. Program: | 55 °C to 285 °C at 10 °C/min (hold 10 min) |
PTV Splitless | |
Purge Flow: | 15 mL/min |
Oven | |
Oven Temp.: | 50 °C to 280 °C at 10 °C/min (hold 10 min) |
Carrier Gas | He, constant flow |
Linear Velocity: | 60 cm/sec @ 300 °C |
Detector | µ-ECD @ 300 °C |
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Make-up Gas Flow Rate: | 60 mL/min |
Make-up Gas Type: | N2 |
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