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Peaks | |
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1. | Phenanthrene |
2. | Anthracene |
Column | Rxi-17Sil MS, 15 m, 0.25 mm ID, 0.25 µm (cat.# 14120) |
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Standard/Sample | |
Diluent: | Methylene chloride |
Conc.: | 20 ng/µL |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 20:1) |
Liner: | 4 mm split Precision liner w/wool (cat.# 21022) |
Inj. Temp.: | 275 °C |
Split Vent Flow Rate: | 42 mL/min |
Oven | |
Oven Temp.: | 80 °C (hold 1 min) to 320 °C at 15 °C/min (hold 2 min) |
Carrier Gas | H2, constant flow |
Flow Rate: | 2 mL/min |
Detector | FID @ 340 °C |
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Constant Column + Constant Make-up: | 50 mL/min |
Make-up Gas Type: | N2 |
Data Rate: | 20 Hz |
Instrument | Agilent/HP6890 GC |
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