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Peaks | |
---|---|
1. | 1,2,3-Trimethylbenzene |
2. | Naphthalene |
3. | 2-Methylnaphthalene |
4. | 2-Fluorobiphenyl |
5. | Acenaphthalene |
6. | 2-Bromonaphthalene |
7. | Acenaphthene |
8. | Fluorene |
9. | Phenanthrene |
10. | Anthracene |
Peaks | |
---|---|
11. | o-Terphenyl |
12. | Fluoranthene |
13. | Pyrene |
14. | Benzo[a]anthracene |
15. | Chrysene |
16. | Benzo[b]fluoranthene |
17. | Benzo[k]fluoranthene |
18. | Benzo[a]pyrene |
19. | Indeno[1,2,3-cd]pyrene |
20. | Dibenzo[a,h]anthracene |
21. | Benzo[ghi]perylene |
Column | Rtx-5, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10224) |
---|---|
Standard/Sample | NJDEP EPH 10/08 Rev.2 aliphatics (cat.# 30540) |
NJDEP EPH 10/08 Rev.2 aromatics (cat.# 30541) | |
MA EPH surrogate spike mix (cat.# 31479) | |
MA fractionation surrogate spike mix (cat.# 31480) | |
Diluent: | Hexane |
Conc.: | 200 ppm |
Injection | |
Inj. Vol.: | 1 µL splitless (hold 1.5 min) |
Liner: | Gooseneck splitless (4 mm) w/wool (cat.# 22406) |
Inj. Temp.: | 280 °C |
Purge Flow: | 40 mL/min |
Oven | |
Oven Temp.: | 60 °C (hold 1 min) to 300 °C at 12 °C/min to 330 °C at 6 °C/min (hold 2 min) |
Carrier Gas | He, constant pressure (18 psi, 124.1 kPa) |
Temp.: | 60 °C |
Detector | FID @ 330 °C |
---|---|
Make-up Gas Flow Rate: | 40 mL/min |
Make-up Gas Type: | N2 |
Instrument | HP5890 GC |
Sample Preparation | A fractionation calibration check standard for the NJDEP EPH method was prepared and fractionated according to the method. See chromatogram GC_EV1208 for aliphatic fraction. |
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