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0.5 ng Semivolatile Organics with Appendix IX on Rxi-5Sil MS by U.S. EPA Method 8270

GC_EV1269
Peaks
1.1,4-Dioxane-d8 (IS)
2.1,4-Dioxane
3.N-Nitrosodimethylamine
4.Pyridine
5.Ethyl methacrylate
6.2-Picoline
7.N-Nitrosomethylethylamine
8.Methyl methanesulfonate
9.2-Fluorophenol (SS)
10.N-Nitrosodiethylamine
11.Ethyl methanesulfonate
12.Benzaldehyde
13.Phenol-d6 (SS)
14.Phenol
15.Aniline
16.Bis(2-chloroethyl) ether
17.Pentachloroethane
18.2-Chlorophenol
19.1,3-Dichlorobenzene
20.1,4-Dichlorobenzene-D4 (IS)
21.1,4-Dichlorobenzene
22.Benzyl alcohol
23.1,2-Dichlorobenzene
24.2-Methylphenol
25.Bis(2-Chloroisopropyl)ether
26.N-Nitrosopyrrolidine
27.3-Methylphenol
28.4-Methylphenol
29.Acetophenone
30.N-Nitrosodipropylamine
31.4-Nitrosomorpholine
32.o-Toluidine
33.Hexachloroethane
34.Nitrobenzene-D5 (SS)
35.Nitrobenzene
36.N-Nitrosopiperidine
37.Isophorone
38.2-Nitrophenol
39.2,4-Dimethylphenol
40.Bis(2-chloroethoxy)methane
41.Benzoic acid
42.2,4-Dichlorophenol
43.α,α-Dimethylphenethylamine
44.1,2,4-Trichlorobenzene
45.Naphthalene-D8 (IS)
46.Naphthalene
47.4-Chloroaniline
48.2,6-Dichlorophenol
Peaks
49.Hexachloropropene
50.Hexachlorobutadiene
51.N-Nitrosobutylamine
52.Caprolactam
53.1,4-Phenylenediamine
54.4-Chloro-3-methylphenol
55.Isosafrole (isomer)
56.2-Methylnaphthalene
57.1-Methylnaphthalene
58.Hexachlorocyclopentadiene
59.1,2,4,5-Tetrachlorobenzene
60.Isosafrole (isomer)
61.2,4,6-Trichlorophenol
62.2,4,5-Trichlorophenol
63.2-Fluorobiphenyl (SS)
64.Safrole
65.Biphenyl
66.2-Chloronaphthalene
67.1-Chloronaphthalene
68.Diphenyl ether
69.2-Nitroaniline
70.1,4-Naphthoquinone
71.1,4-Dinitrobenzene
72.Dimethyl phthalate
73.1,3-Dinitrobenzene
74.2,6-Dinitrotoluene
75.1,2-Dinitrobenzene
76.Acenaphthylene
77.3-Nitroaniline
78.Acenaphthene-d10 (IS)
79.Acenaphthene
80.2,4-Dinitrophenol
81.4-Nitrophenol
82.Pentachlorobenzene
83.2,4-Dinitrotoluene
84.Dibenzofuran
85.1-Naphthalamine
86.2,3,5,6-Tetrachlorophenol
87.2,3,4,6-Tetrachlorophenol
88.2-Naphthalamine
89.Diethyl phthalate
90.4-Chlorophenyl phenyl ether
91.Fluorene
92.2-Methyl-5-nitroaniline
93.4-Nitroaniline
94.4,6-Dinitro-2-methylphenol
95.N-nitrosodiphenylamine (as diphenylamine)
96.1,2-Diphenylhydrazine (as azobenzene)
Peaks
97.2,4,6-Tribromophenol (SS)
98.1,3,5-Trinitrobenzene
99.Diallate
100.Phenacetin
101.4-Bromophenyl phenyl ether
102.Hexachlorobenzene
103.Atrazine
104.4-Aminobiphenyl
105.Pentachlorophenol
106.Pentachloronitrobenzene
107.Propyzamide
108.Phenanthrene-D10 (IS)
109.Phenanthrene
110.Anthracene
111.Carbazole
112.di-n-Butyl phthalate
113.4-Nitroquinoline 1-oxide
114.Methapyriline
115.Isodrin
116.Fluoranthene
117.Benzidine
118.Pyrene-d10 (SS)
119.Pyrene
120.Aramite (isomer)
121.p-Terphenyl-d14 (SS)
122.Aramite (isomer)
123.Dimethylaminoazobenzene
124.Chlorobenzilate
125.3,3'-Dimethylbenzidine
126.Butyl benzyl phthalate
127.Kepone
128.Bis(2-ethylhexyl) adipate
129.2-Acetylaminofluorene
130.3,3'-Dichlorobenzidine
131.Benz[a]anthracene
132.Chrysene-D12 (IS)
133.Bis(2-ethylhexyl)phthalate
134.Chrysene
135.Di-n-octyl phthalate
136.7,12-Dimethylbenzo[a]anthracene
137.Benzo[b]fluoranthene
138.Benzo[k]fluoranthene
139.Benzo[a]pyrene
140.Perylene-D12 (IS)
141.3-Methylcholanthrene
142.Dibenzo[a,j]acridine
143.Indeno[1,2,3-cd]pyrene
144.Dibenz[a,h]anthracene
145.Benzo[ghi]perylene
ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Standard/Sample8270 MegaMix (cat.# 31850)
8270 Benzidines mix (cat.# 31852)
Benzoic acid (cat.# 31879)
Revised B/N surrogate mix (cat.# 31888)
Acid surrogate mix (4/89 SOW) (cat.# 31063)
Revised SV internal standard mix (cat.# 31886)
Appendix IX mix #1 (cat.# 31625)
Appendix IX mix #2 (cat.# 31806)
Diluent:Dichloromethane
Conc.:0.5 µg/mL (IS/SS 20 μg/mL)
Injection
Inj. Vol.:1 µL pulsed splitless (hold 0.59 min)
Liner:Premium 4 mm single taper/gooseneck w/wool (cat.# 23303.1)
Inj. Temp.:270 °C
Pulse Pressure:30 psi (206.8kPa)
Pulse Time:0.64 min
Purge Flow:100 mL/min
Oven
Oven Temp.:40 °C (hold 1 min) to 280 °C at 25 °C/min to 320 °C at 5 °C/min (hold 1 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Source Temp.:276 °C
Quad Temp.:150 °C
Electron Energy:70 eV
Solvent Delay Time:2.19 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
Scan Rate:5.36 scans/sec
InstrumentAgilent 7890A GC & 5975C MSD
Notes7890 Siltek-treated EZ Twist Top split/splitless injection port (cat.# 22178)
Flip Seal dual Vespel ring inlet seal (cat.# 23411)
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