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PCB Congener Mix (EPA Method 8082A) on the Rtx-PCB Column

ColumnRtx-PCB, 20 m, 0.18 mm ID, 0.18 µm (cat.# 41302)
Standard/SamplePCB congener mix, Method 8082A (cat.# 32416)
Diluent:Isooctane
Conc.:50 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 10:1)
Liner:Premium 4 mm Precision liner w/wool (cat.# 23305.5)
Inj. Temp.:250 °C
Oven
Oven Temp.:120 °C (hold 0.1 min) to 330 °C at 6.8 °C/min (hold 1 min)
Carrier GasHe, constant flow
Flow Rate:1 mL/min
DetectorMS-scan (positive ion chemical ionization emulating EI [EI-CI source.u])
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
1350-5505.6
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Source Type:CI
Source Temp.:300 °C
Quad Temp.:200 °C
Ionization Mode:CI(pos)
InstrumentAgilent 7890B GC & 5977A MSD