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Peaks | tR (min) | |
---|---|---|
1. | 1,4-Dioxane-D8 (IS) | 1.98 |
2. | N-Nitrosodimethylamine | 2.15 |
3. | Pyridine | 2.18 |
4. | 2-Fluorophenol (SS) | 2.87 |
5. | Phenol-D6 (SS) | 3.48 |
6. | Phenol | 3.49 |
7. | Aniline | 3.54 |
8. | bis-(2-chloroethyl)ether | 3.57 |
9. | 2-Chlorophenol | 3.62 |
10. | 1,3-Dichlorobenzene | 3.74 |
11. | 1,4-Dichlorobenzene-D4 (IS) | 3.76 |
12. | 1,4-Dichlorobenzene | 3.77 |
13. | Benzyl Alcohol | 3.86 |
14. | 1,2-Dichlorobenzene | 3.92 |
15. | 2-Methylphenol | 3.95 |
16. | Bis(2-Chloroisopropyl)ether | 3.98 |
17. | 4-Methylphenol | 4.06 |
18. | 3-Methylphenol | 4.06 |
19. | N-Nitrosodi-N-propylamine | 4.09 |
20. | Hexachloroethane | 4.17 |
21. | Nitrobenzene-D5 (SS) | 4.21 |
22. | Nitrobenzene | 4.22 |
23. | Isophorone | 4.41 |
24. | 2-Nitrophenol | 4.49 |
25. | 2,4-Dimethylphenol | 4.5 |
26. | Benzoic acid | 4.54 |
27. | Bis(2-chloroethoxy)methane | 4.58 |
28. | 2,4-Dichlorophenol | 4.67 |
29. | 1,2,4-Trichlorobenzene | 4.76 |
30. | Naphthalene-D8 (IS) | 4.79 |
31. | Naphthalene | 4.81 |
Peaks | tR (min) | |
---|---|---|
32. | 4-Chloroaniline | 4.86 |
33. | Hexachlorobutadiene | 4.96 |
34. | 4-Chloro-3-methylphenol | 5.26 |
35. | 2-Methylnaphthalene | 5.4 |
36. | 1-Methylnaphthalene | 5.49 |
37. | Hexachlorocyclopentadiene | 5.6 |
38. | 2,4,6-Trichlorophenol | 5.66 |
39. | 2,4,5-Trichlorophenol | 5.69 |
40. | 2-Fluorobiphenyl (SS) | 5.73 |
41. | 2-Chloronaphthalene | 5.82 |
42. | 2-Nitroaniline | 5.93 |
43. | 1,4-Dinitrobenzene | 6.02 |
44. | Dimethyl phthalate | 6.11 |
45. | 1,3-Dinitrobenzene | 6.12 |
46. | 2,6-Dinitrotoluene | 6.17 |
47. | Acenaphthylene | 6.19 |
48. | 1,2-Dinitrobenzene | 6.23 |
49. | 3-Nitroaniline | 6.29 |
50. | Acenaphthene-D10 (IS) | 6.33 |
51. | Acenaphthene | 6.35 |
52. | 2,4-Dinitrophenol | 6.38 |
53. | 4-Nitrophenol | 6.42 |
54. | Dibenzofuran | 6.49 |
55. | 2,4-Dinitrotoluene | 6.51 |
56. | 2,3,5,6-Tetrachlorophenol | 6.59 |
57. | 2,3,4,6-Tetrachlorophenol | 6.63 |
58. | Diethyl Phthalate | 6.72 |
59. | 4-Chlorophenyl phenyl ether | 6.79 |
60. | Fluorene | 6.8 |
61. | 4-Nitroaniline | 6.83 |
62. | 4,6-Dinitro-2-methylphenol | 6.87 |
Peaks | tR (min) | |
---|---|---|
63. | N-Nitrosodiphenylamine (as Diphenylamine) | 6.89 |
64. | N,N'-Diphenylhydrazine (as Azobenzene) | 6.93 |
65. | 2,4,6-Tribromophenol (SS) | 7.02 |
66. | 4-Bromophenyl phenyl ether | 7.22 |
67. | Hexachlorobenzene | 7.36 |
68. | Pentachlorophenol | 7.51 |
69. | Phenanthrene-D10 (IS) | 7.62 |
70. | Phenanthrene | 7.64 |
71. | Anthracene | 7.68 |
72. | Carbazole | 7.82 |
73. | di-n-Butyl phthalate | 8.16 |
74. | Fluoranthene | 8.73 |
75. | Benzidine | 8.85 |
76. | Pyrene-D10 (SS) | 8.95 |
77. | Pyrene | 8.97 |
78. | p-Terphenyl-D14 (SS) | 9.14 |
79. | 3,3'-Dimethylbenzidine | 9.74 |
80. | Butyl benzyl phthalate | 9.79 |
81. | Bis(2-ethylhexyl) adipate | 9.89 |
82. | 3,3'-Dichlorobenzidine | 10.6 |
83. | Benz[a]anthracene | 10.62 |
84. | Chrysene-D12 (IS) | 10.65 |
85. | Chrysene | 10.69 |
86. | Bis(2-ethylhexyl) phthalate | 10.8 |
87. | Di-n-octyl phthalate | 12.14 |
88. | Benzo[b]fluoranthene | 12.93 |
89. | Benzo[k]fluoranthene | 12.99 |
90. | Benzo[a]pyrene | 13.77 |
91. | Perylene-D12 (IS) | 13.93 |
92. | Indeno[1,2,3-cd]pyrene | 16.56 |
93. | Dibenz[a,h]anthracene | 16.62 |
94. | Benzo[ghi]perylene | 17 |
Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) |
---|---|
Standard/Sample | Revised SV internal standard mix (cat.# 31886) |
Revised B/N surrogate mix (cat.# 31888) | |
Acid surrogate mix (4/89 SOW) (cat.# 31063) | |
8270 MegaMix (cat.# 31850) | |
8270 Benzidines mix (cat.# 31852) | |
Benzoic acid (cat.# 31879) | |
Diluent: | Dichloromethane |
Conc.: | 5.0 ng/µL (IS and SS concentrations are 20 ng/µL) |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 10:1) |
Liner: | Premium 4 mm Precision liner w/wool (cat.# 23305.5) |
Inj. Temp.: | 275 °C |
Oven | |
Oven Temp.: | 50 °C (hold 0.5 min) to 265 °C at 28 °C/min to 285 °C at 3 °C/min to 330 °C at 20 °C/min (hold 5 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.44 mL/min |
Detector | MS | ||||||||
---|---|---|---|---|---|---|---|---|---|
Mode: | Scan | ||||||||
Scan Program: | |||||||||
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Transfer Line Temp.: | 280 °C | ||||||||
Analyzer Type: | Quadrupole | ||||||||
Source Type: | Extractor | ||||||||
Extractor Lens: | 9mm ID | ||||||||
Source Temp.: | 350 °C | ||||||||
Quad Temp.: | 200 °C | ||||||||
Electron Energy: | 70 eV | ||||||||
Tune Type: | DFTPP | ||||||||
Ionization Mode: | EI | ||||||||
Instrument | Agilent 7890B GC & 5977A MSD |