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|Column||Rtx-CLPesticides, 30 m, 0.32 mm ID, 0.32 µm (cat.# 11141)|
|Decachlorobiphenyl (BZ #209) (cat.# 32029)|
|Inj. Vol.:||4 µL splitless (hold 0.75 min)|
|Liner:||Topaz 4.0 mm ID single taper inlet liner w/wool (cat.# 23303)|
|Inj. Temp.:||250 °C|
|Purge Flow:||50 mL/min|
|Oven Temp.:||90 °C (hold 0.5 min) to 330 °C at 25 °C/min (hold 2 min)|
|Carrier Gas||He, constant flow|
|Flow Rate:||3.5 mL/min|
|Detector||Micro-ECD @ 340 °C|
|Make-up Gas Flow Rate:||50 mL/min|
|Make-up Gas Type:||N2|
|Data Rate:||50 Hz|
|Sample Preparation||Conditioned a Resprep CarboPrep Plus SPE cartridge (cat.# 25845) by adding one cartridge volume of hexane:acetone (90:10) and letting it stand for five minutes before drawing the solvent down to frit level. Then, 1 mL of sample extract was loaded onto the cartridge and eluted with 9 mL of hexane:acetone (90:10).|
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