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Peaks | |
---|---|
1. | Squalene (IS) |
2. | Cholesterol |
3. | β-Sitosterol |
4. | Diglycerides |
5. | Triglycerides |
Column | Rtx-65TG, 30 m, 0.25 mm ID, 0.10 µm (cat.# 17008) |
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Standard/Sample | 50 μg/mL fat extract from egg in diethyl ether solution with 3000 ppm squalene (IS) |
Injection | |
Inj. Vol.: | 0.5 µL PTV split (split ratio 80:1) |
Inlet Temp. Program: | 70 °C (hold 12 min) to 370 °C at 99 °C/min (hold 5 min) |
Oven | |
Oven Temp.: | 220 °C (hold 2 min) to 360 °C at 5 °C/min (hold 5 min) |
Carrier Gas | H2, constant flow |
Flow Rate: | 1.5 mL/min |
Detector | FID @ 370 °C |
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Acknowledgement | Daniele Naviglio, Professor, Analytical Chemist, and Fabiana Pizzolongo, Ph.D., Food Technologist; Dipartimento di Scienza degli Alimenti – Università degli Studi di Napoli “Federico II” – Via Università, 100 - 80055 Portici (NA) – Italia |
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