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Peaks | tR (min) | |
---|---|---|
1. | α-Pinene | 1.471 |
2. | Camphene | 1.542 |
3. | β-Pinene | 1.616 |
4. | β-Myrcene | 1.679 |
5. | D-Limonene | 1.805 |
6. | Eucalyptol | 1.840 |
7. | β-Ocimene | 1.857 |
8. | α-Ocimene | 1.916 |
9. | γ-Terpinene | 1.933 |
10. | p-Cymene | 2.014 |
11. | Terpinolene | 2.061 |
12. | Octenyl acetate | 2.364 |
13. | Hexyl butyrate | 2.554 |
Peaks | tR (min) | |
---|---|---|
14. | Camphor | 3.154 |
15. | Linalool | 3.188 |
16. | Linalyl acetate | 3.303 |
17. | Geranyl butyrate | 3.559 |
18. | 4-Carvomenthenol | 3.575 |
19. | Caryophyllene | 3.636 |
20. | Lavandulol | 3.964 |
21. | α-Terpineol | 4.098 |
22. | Borneol | 4.147 |
23. | β-Cubebene | 4.286 |
24. | Geranyl acetate | 4.487 |
25. | Lavandulyl acetate | 4.512 |
26. | Geraniol | 4.994 |
Column | Rtx-Wax, 30 m, 0.32 mm ID, 0.25 µm (cat.# 12424) |
---|---|
Standard/Sample | Lavender oil |
Diluent: | Acetone |
Conc.: | 5% |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 100:1) |
Liner: | Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305) |
Inj. Temp.: | 230 °C |
Oven | |
Oven Temp.: | 100 °C (hold 0.5 min) to 250 °C at 16 °C/min (hold 10 min) |
Carrier Gas | H2, constant flow |
Flow Rate: | 2 mL/min |
Detector | FID @ 250 °C |
---|---|
Constant Column + Constant Make-up: | 52 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 400 mL/min |
Data Rate: | 50 Hz |
Instrument | Agilent 7890A GC |
Notes | All peaks were identified using the NIST MS EI spectra library (2005). |
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