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Peaks | tR (min) | |
---|---|---|
1. | Camphene | 1.308 |
2. | 6-Methyl-5-heptene-2-one | 1.352 |
3. | β-Ocimene | 1.549 |
4. | D-Limonene | 1.570 |
5. | α-Ocimene | 1.598 |
6. | 4-Nonanone | 1.704 |
7. | Linalool | 1.849 |
Peaks | tR (min) | |
---|---|---|
8. | Z-Citral | 2.697 |
9. | Geraniol | 2.741 |
10. | E-Citral | 2.893 |
11. | Geranyl acetate | 3.553 |
12. | Caryophyllene | 3.943 |
13. | α-Caryophyllene | 4.057 |
14. | α-Amorphene | 4.553 |
15. | δ-Cadinene | 4.553 |
Column | Rxi-5Sil MS, 20 m, 0.18 mm ID, 0.18 µm (cat.# 43602) |
---|---|
Standard/Sample | Lemongrass oil |
Diluent: | Acetone |
Conc.: | 5% |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 100:1) |
Liner: | Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 100 °C (hold 0.25 min) to 320 °C at 17.5 °C/min (hold 10 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1.01 mL/min |
Detector | MS | ||||||||
---|---|---|---|---|---|---|---|---|---|
Mode: | Scan | ||||||||
Scan Program: | |||||||||
| |||||||||
Transfer Line Temp.: | 300 °C | ||||||||
Analyzer Type: | Quadrupole | ||||||||
Source Type: | Inert | ||||||||
Source Temp.: | 230 °C | ||||||||
Quad Temp.: | 150 °C | ||||||||
Instrument | Agilent 7890A GC & 5975C MSD | ||||||||
Notes | All peaks were identified using the NIST MS EI spectra library (2005). |
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