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QuEChERS Performance Standards Kit Pesticides on Rxi-5ms

GC_FS0530
PeakstR (min)
1.Methamidophos8.20
2.Dichlorvos8.61
3.Mevinphos11.62
4.Acephate11.66
5.o-Phenylphenol12.93
6.Omethoate14.07
7.Dimethoate16.02
8.gamma-BHC16.53
9.Diazinon17.04
10.Chlorothalonil17.28
11.Vinclozolin18.21
12.Carbaryl18.31
13.Metalaxyl18.54
PeakstR (min)
14.Methiocarb18.88
15.Pirimiphos methyl18.95
16.Dichlofluanid19.09
17.Malathion19.17
18.Fenthion19.37
19.Chlorpyrifos19.42
20.Cyprodinil20.03
21.Thiabendazole20.28
22.Captan20.40
23.Folpet20.56
24.Imazalil21.49
25.Myclobutanil21.83
26.Endrin22.22
PeakstR (min)
27.Endosulfan sulfate23.42
28.Fenhexamid23.47
29.4,4'-DDT23.50
30.Propargite*23.92
31.Iprodione24.41
32.Dicofol24.83
33.Bifenthrin24.72
34.Fenpropathrin24.85
35.Phosalone25.48
36.Azinphos-methyl25.48
37.cis-Permethrin26.83
38.trans-Permethrin26.98
39.Coumaphos27.10
40.Deltamethrin29.95
*Propargite isomers are listed as one peak.
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
Standard/SampleQuEChERS performance standards kit (cat.# 31152)
Diluent:Acetonitrile
Conc.:1 ng/µL
Injection
Inj. Vol.:1 µL splitless (hold 1 min)
Inj. Temp.:250 °C
Oven
Oven Temp.:70 °C (hold 1 min) to 330 °C at 8 °C/min (hold 6.5 min)
Carrier GasHe, constant flow
Flow Rate:1.4 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)		Scan Range
(amu)		Scan Rate
(scans/sec)
16.545-5503.3
Transfer Line Temp.:320 °C
Analyzer Type:Quadrupole
Source Temp.:250 °C
Electron Energy:70 eV
Solvent Delay Time:6.5 min
Tune Type:PFTBA
Ionization Mode:EI
InstrumentThermo Scientific TSQ 8000 Triple Quadrupole GC-MS
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