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GC Multiresidue Pesticide Standard #4-ONP on Rxi-5ms by GC-MS

GC_FS0603
PeakstR (min)
1.Allidochlor6.83
2.Pebulate9.37
3.N-(2,4-Dimethylphenyl)formamide9.63
4.Propachlor11.51
5.Cycloate11.80
6.Diallate 1*12.60
7.Diallate 2*12.80
8.Clomazone (Command)13.36
9.Propyzamide13.73
10.Triallate14.28
11.Propanil14.82
12.Dimethachlor14.87
13.Acetochlor15.03
14.Alachlor15.26
PeakstR (min)
15.Propisochlor15.35
16.Linuron15.79
17.Metolachlor16.10
18.Diphenamid16.61
19.Metazachlor16.91
20.Flutolanil18.07
21.Pretilachlor18.29
22.Oxadiazon18.40
23.Norflurazon19.93
24.Methoxychlor21.25
25.Fenpropathrin21.30
26.Tebufenpyrad21.37
27.Pyridaben23.30
28.Fluquinconazole23.41
29.Prochloraz23.48
*Diallate isomers numbered according to elution order.
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
Standard/SampleGC multiresidue pesticide standard #4-ONP (cat.# 32566)
Diluent:Toluene
Conc.:100 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 50:1)
Liner:Premium 4.0 mm ID Precision inlet liner w/wool (cat.# 23305.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:90 °C (hold 1 min) to 330 °C at 8.5 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.4 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)		Scan Range
(amu)		Scan Rate
(scans/sec)
1555-5507
Transfer Line Temp.:290 °C
Analyzer Type:Quadrupole
Source Temp.:325 °C
Electron Energy:70 eV
Solvent Delay Time:5 min
Ionization Mode:EI
InstrumentThermo Scientific TSQ 8000 Triple Quadrupole GC-MS
NotesReconstructed chromatogram from select ions.
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