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Terpenes MegaMix #1 & #2 on Rxi-1301Sil MS

GC_GN1210
PeakstR (min)
1.alpha-Pinene7.39
2.Camphene8.00
3.(-)-beta-Pinene9.07
4.Sabinene9.07
5.Beta-myrcene9.89
6.3-Carene10.30
7.R-(-)-alpha-Phellandrene10.30
8.alpha-Terpinene10.84
9.D-Limonene11.26
10.m-Isopropyltoluene11.32
11.p-Cymene11.51
12.Eucalyptol11.64
13.cis-beta-Ocimene11.86
14.o-Isopropyltoluene12.03
15.trans-beta-Ocimene12.37
16.gamma-Terpinene12.56
17.Terpinolene13.74
18.Sabinene hydrate14.57
19.(1R)-(-)-Fenchone*15.44
20.Linalool16.14
21.(-)-alpha-Thujone*16.45
PeakstR (min)
22.(1R)-endo-(+)-Fenchyl alcohol17.09
23.(-)-Isopulegol17.81
24.Camphor*18.22
25.l-Menthone*18.61
26.Isoborneol18.81
27.Terpinen-4-ol19.08
28.D-isomenthone*19.11
29.(+)-Borneol19.39
30.L(-)-Borneol19.39
31.Menthol19.52
32.alpha-Terpineol20.23
33.Safranal*20.58
34.Octyl acetate*20.71
35.Nerol21.79
36.(-)-Verbenone*21.81
37.d-Valerolactam*21.92
38.Citronellol21.99
39.(R)-(+)-Pulegone*22.07
40.(S)-(+)-Carvone*22.43
41.cis-Citral*22.58
42.Geraniol22.70
PeakstR (min)
43.Piperitone*22.97
44.Isobornyl acetate*23.18
45.trans-Citral*23.47
46.Thymol24.87
47.Carvacrol25.08
48.(-)-alpha-Cedrene25.47
49.Geranyl acetate*25.47
50.Beta-caryophyllene25.75
51.alpha-Humulene26.46
52.trans-beta-Farnesene26.46
53.Valencene27.12
54.cis-Nerolidol28.34
55.trans-Nerolidol28.81
56.(-)-Caryophyllene oxide*29.34
57.(-)-Guaiol29.41
58.Cedrol29.53
59.(-)-alpha-Bisabolol30.66
60.Farnesol 130.92
61.Farnesol 231.25
62.Phytane (2,6,10,14-Tetramethylhexadecane)31.78
63.(+)-Nootkatone*32.97
64.Squalene37.73
All compounds at 10 µg/mL. Compounds with an * are from Terpenes MegaMix #2 (cat.# 34143).
ColumnRxi-1301Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 16094)
Standard/SampleTerpenes MegaMix #1 (cat.# 34142)
Terpenes MegaMix #2 (cat.# 34143)
Diluent:Isopropanol
Conc.:10 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 25:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/ wool (cat.# 23305)
Inj. Temp.:280 °C
Split Vent Flow Rate:45 mL/min
Oven
Oven Temp.:40 °C (hold 0.5 min) to 100 °C at 3 °C/min to 200 °C at 8 °C/min to 300 °C at 25 °C/min (hold 3 min)
Carrier GasHe, constant flow
Flow Rate:1.8 mL/min
Detector5977B
Scan Program:
GroupStart Time
(min)		Scan Range
(amu)		Scan Rate
(scans/sec)
16.535-3502.3
Transfer Line Temp.:300 °C
Analyzer Type:Quadrupole
Source Type:HES
Source Temp.:325 °C
Quad Temp.:200 °C
Electron Energy:70 eV
Solvent Delay Time:6.5 min
Tune Type:BFB
Ionization Mode:EI
InstrumentAgilent 7890B GC & 5977B MSD
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