Terpenes MegaMix #1 on Rxi-1301Sil MS

	Peaks	t_R (min)
31.	Thymol	24.87
32.	Carvacrol	25.08
33.	(-)-alpha-Cedrene	25.47
34.	Beta-caryophyllene	25.75
35.	alpha-Humulene	26.46
36.	trans-beta-Farnesene	26.46
37.	Valencene	27.12
38.	cis-Nerolidol	28.34
39.	trans-Nerolidol	28.81
40.	(-)-Guaiol	29.41
41.	Cedrol	29.53
42.	(-)-alpha-Bisabolol	30.66
43.	Farnesol 1	30.92
44.	Farnesol 2	31.25
45.	Phytane (2,6,10,14-Tetramethylhexadecane)	31.78
46.	Squalene	37.73

All compounds at 10 µg/mL.

Injection
Column	Rxi-1301Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 16094)
Standard/Sample	Terpenes MegaMix #1 (cat.# 34142)


Diluent:	Isopropanol
Conc.:	10 µg/mL
Inj. Vol.:	1 µL split (split ratio 25:1)
Liner:	Topaz 4.0 mm ID Precision inlet liner w/ wool (cat.# 23305)
Inj. Temp.:	280 °C
Split Vent Flow Rate:	45 mL/min
Oven
Oven Temp.:	40 °C (hold 0.5 min) to 100 °C at 3 °C/min to 200 °C at 8 °C/min to 300 °C at 25 °C/min (hold 3 min)
Carrier Gas	He, constant flow
Flow Rate:	1.8 mL/min

Detector

5977B

Scan Program:

Group	Start Time (min)	Scan Range (amu)	Scan Rate (scans/sec)
1	6.5	35-350	2.3

Transfer Line Temp.:

300 °C

Analyzer Type:

Quadrupole

Source Type:

HES

Source Temp.:

325 °C

Quad Temp.:

200 °C

Electron Energy:

70 eV

Solvent Delay Time:

6.5 min

Tune Type:

BFB

Ionization Mode:

Instrument

Agilent 7890B GC & 5977B MSD

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