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Helium/Hydrogen Separation using Rt-Msieve 5A

GC_MS01136
Peaks
1.Helium
2.Hydrogen
ColumnRt-Msieve 5A, 30 m, 0.53 mm ID, 50 µm (cat.# 19723)
Standard/SampleHelium/hydrogen gas mixture
Injection
Inj. Vol.:25 µL split (split ratio 10:1)
Liner:2 mm split Precision liner w/wool (cat.# 20823)
Inj. Temp.:200 °C
Split Vent Flow Rate:40 mL/min
Oven
Oven Temp.:30 °C
Carrier GasN2, constant pressure (7.0 psi, 48.3 kPa)
Linear Velocity:38 cm/sec @ 30 °C
DetectorTCD @ 200 °C
Make-up Gas Type:N2
Data Rate:20 Hz
Sensitivity Mode:N2/Ar
InstrumentHP5890 GC