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Derivatized B100 and Internal Standards on MXT-Biodiesel TG with 2 m Integra Gap

ColumnMXT-Biodiesel TG 13 m, 0.53 mm ID, 0.16 µm with built-in 2 m Integra-Gap (total column length 15 m)
Standard/SampleB100 + IS butanetriol & tricaprin derivatized with MSTFA as per ASTM D-6584
Inj. Vol.:1.0 µL cold on-column
Temp. Program:oven track
Oven Temp.:50 °C (hold 1 min) to 180 °C at 15 °C/min to 230 °C at 7 °C/min to 430 °C at 30 °C/min (hold 5 min)
Carrier GasH2, constant flow
Flow Rate:4 mL/min
DetectorFID @ 430 °C
InstrumentShimadzu 2010 GC
Notes(Data acquired on prototype column, similar column to cat# 70290)