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Total Glycerin in Biodiesel on MXT-Biodiesel TG

GC_PC00969
ColumnMXT-Biodiesel TG, 14 m w/2 m Integra-Gap (16 m total length), 0.53 mm ID, 0.16 µm (cat.# 70289)
SampleBiodiesel (B100), derivatized
Diluent:Heptane
Injection
Inj. Vol.:1 µL cold on-column
Temp. Program:Oven track
Oven
Oven Temp.:50 °C (hold 1 min) to 180 °C at 15 °C/min to 230 °C at 7 °C/min to 380 °C at 30 °C/min (hold 5 min)
Carrier GasH2, constant flow
Flow Rate:4 mL/min
DetectorFID @ 380 °C