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Column | Rt-QS-BOND, 30 m, 0.53 mm ID, 20 µm (cat.# 19738) |
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Standard/Sample | solvent mix |
Diluent: | DMSO:water, 60:40 (v/v) |
Conc.: | 100-1000 µg/mL |
Injection | |
Inj. Vol.: | 1.0 µL split (split ratio 5:1) |
Liner: | Gooseneck Splitless (4mm) Siltek® (cat.# 20798-214.1) |
Inj. Temp.: | 240 °C |
Oven | |
Oven Temp.: | 40 °C (hold 0.5 min) to 120 °C at 15 °C/min to 200 °C at 5 °C/min (hold 10 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 5.7 mL/min @ 40 °C |
Detector | FID @ 240 °C |
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