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Peaks | |
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1. | Methane |
2. | Ethane |
3. | Ethylene |
4. | Propane |
5. | Cyclopropane |
6. | Propylene |
7. | Acetylene |
8. | Isobutane |
9. | Propadiene |
Peaks | |
---|---|
10. | n-Butane |
11. | trans-2-Butene |
12. | 1-Butene |
13. | Isobutylene |
14. | cis-2-Butene |
15. | iso-Pentane |
16. | Methylacetylene |
17. | n-Pentane |
18. | 1,3-Butadiene |
Column | Rt-Alumina BOND/KCl *, 50 m, 0.53 mm ID, 10 µm (cat.# 19760) |
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Standard/Sample | Ethylene gas plus C1 through C5 hydrocarbons |
Injection | |
Inj. Vol.: | 1 µL split |
Liner: | 2 mm splitless (cat.# 20712) |
Inj. Temp.: | 200 °C |
Split Vent Flow Rate: | 60 ml/min |
Oven | |
Oven Temp.: | 35 °C (hold 2 min) to 190 °C at 4 °C/min (hold 15 min) |
Carrier Gas | He, constant pressure (8.0 psi, 55.2 kPa) |
Linear Velocity: | 25.4 cm/sec @ 35 °C |
Detector | FID @ 200 °C |
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Make-up Gas Type: | N2 |
Data Rate: | 20 Hz |
Instrument | HP5890 GC |
Notes | * Rt-Alumina BOND/KCl, 50 m, 0.53 mm ID, 10.0 μm (cat.# 19760) in series with an Rtx-1, 30 m, 0.53 mm ID, 5.0 μm (cat.# 10179) connected using a universal Press-Tight connector (cat. # 20401). (conditions as per ASTM D6159-97) |