Hydrocarbons (C5-C106) on MXT-1HT SimDist at 450 °C

GC_PC1164

	Peaks	t_R (min)
1.	C5	--
2.	C6	--
3.	C7	--
4.	C8	--
5.	C9	--
6.	C10	--
7.	C11	--
8.	C12	0.938
9.	C13	1.586
10.	C14	2.425
11.	C15	3.365
12.	C16	4.332
13.	C17	5.290
14.	C18	6.217
15.	C20	7.966
16.	C22	9.566
17.	C24	11.051
18.	C26	12.426
19.	C28	13.689

	Peaks	t_R (min)
20.	C30	14.897
21.	C32	16.035
22.	C34	17.110
23.	C36	18.133
24.	C38	19.108
25.	C40	20.096
26.	C42	20.923
27.	C44	21.759
28.	C46	22.556
29.	C48	23.317
30.	C50	24.051
31.	C52	24.752
32.	C54	25.422
33.	C56	26.079
34.	C58	26.701
35.	C60	27.305
36.	C62	27.878
37.	C64	28.439
38.	C66	28.975

	Peaks	t_R (min)
39.	C68	29.499
40.	C70	30.002
41.	C72	30.489
42.	C74	30.906
43.	C76	31.414
44.	C78	31.862
45.	C80	32.294
46.	C82	32.719
47.	C84	33.132
48.	C86	33.529
49.	C88	33.927
50.	C90	34.310
51.	C92	34.689
52.	C94	35.059
53.	C96	35.423
54.	C98	35.773
55.	C100	36.120
56.	C102	36.463
57.	C104	36.793
58.	C106	37.118

Injection
Column	MXT-1HT SimDist, 5 m, 0.53 mm ID, 0.10 µm (cat.# 70112)
Standard/Sample	Custom C5-C106 hydrocarbon standard
Diluent:	Carbon disulfide
Conc.:	1%
Inj. Vol.:	0.5 µL cold on-column
Temp. Program:	53 °C to 450 °C at 10 °C/min (hold 5 min)
Oven
Oven Temp.:	50 °C to 450 °C at 10 °C/min (hold 5 min)
Carrier Gas	He, constant flow
Flow Rate:	18 mL/min

Detector	FID @ 450 °C
Make-up Gas Flow Rate:	24 mL/min
Constant Column + Constant Make-up:	42 mL/min
Make-up Gas Type:	N₂
Data Rate:	20 Hz
Instrument	Shimadzu 2010 GC

Download PDF