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Peaks | |
---|---|
1. | Isobutane |
2. | n-Butane |
3. | Propadiene |
4. | trans-2-Butene |
5. | 1-Butene |
6. | Isobutylene |
Peaks | |
---|---|
7. | cis-2-Butene |
8. | Isopentane |
9. | n-Pentane |
10. | 1,2-Butadiene |
11. | 1,3-Butadiene |
12. | Methyl acetylene |
Column | Rt-Alumina BOND/MAPD, 50 m, 0.53 mm ID, 10 µm (cat.# 19778) |
---|---|
Standard/Sample | crude 1,3-butadiene |
Diluent: | none |
Injection | |
Inj. Vol.: | 5 µL split |
Liner: | 2 mm ID straight inlet liner (cat.# 20712) |
Inj. Temp.: | 200 °C |
Split Vent Flow Rate: | 45 mL/min |
Oven | |
Oven Temp.: | 70 °C (hold 5 min) to 200 °C at 10 °C/min (hold 10 min) |
Carrier Gas | He, constant pressure (20 psi, 137.9 kPa) |
Temp.: | 70 °C |
Detector | FID @ 200 °C |
---|---|
Make-up Gas Flow Rate: | 30 mL/min |
Make-up Gas Type: | N2 |
Data Rate: | 20 Hz |
Instrument | HP5890 GC |
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