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Peaks | |
---|---|
1. | Amobarbital |
2. | Pentobarbital |
3. | Secobarbital |
4. | Hexobarbital |
5. | Mephobarbital |
6. | Phenobarbital |
Column | 3% OV-17 DA, 100/120 mesh on DiatoSorb WHP, SilcoSmooth tubing, 1 m, 1/8 in OD, 2 mm ID |
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Standard/Sample | Secobarbital (cat.# 34038) |
Hexobarbital (cat.# 34033) | |
Mephobarbital (cat.# 34034) | |
Phenobarbital (cat.# 34037) | |
Pentobarbital (cat.# 34036) | |
Conc.: | 0.2 mg/mL |
Injection | |
Inj. Vol.: | 1 µL on-column |
Liner: | Packed column inlet adaptor kit for 1/4" injection ports (cat.# 21651) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 210 °C (hold 12 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 20 mL/min |
Detector | FID @ 275 °C |
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Instrument | Agilent 7890B GC |
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