Analysis of Glycerol, Mono-, Di-, and Triglycerides in Soy B100 by EN 14105 (2011)

Injection
Column	MXT-Biodiesel TG with 2 m x 0.53 mm ID retention gap, 15 m, 0.32 mm ID, 0.10 µm (cat.# 70291)
Standard/Sample	Soy biodiesel B100
	EN 14105 custom standard 1 (cat.# 572879)
	(s)-(-)-1,2,4-Butanetriol (cat.# 33032)
	MSTFA (N-methyl-N-trimethylsilytrifluoroacetamide) (cat.# 35600)
Diluent:	Heptane
Inj. Vol.:	1 µL cool on-column
Temp. Program:	Oven track
Oven
Oven Temp.:	50 °C (hold 1 min) to 180 °C at 15 °C/min to 230 °C at 7 °C/min to 370 °C at 10 °C/min (hold 5 min)
Carrier Gas	H₂, constant flow
Flow Rate:	7 mL/min

Detector	FID @ 380 °C
Instrument	Agilent 7890A GC
Notes	The sample was derivatized with MSTFA according to the method EN 14105 (2011) procedure.

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