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Methyl Isobutyl Ketone (MIBK) Purity Analysis (ASTM D3329) on Stabilwax

ColumnStabilwax, 30 m, 0.53 mm ID, 1.00 µm (cat.# 10655)
Standard/SampleMethyl isobutyl ketone
Inj. Vol.:0.5 µL split (split ratio 50:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/ wool (cat.# 23305)
Inj. Temp.:250 °C
Oven Temp.:40 °C (hold 3 min) to 220 °C at 10 °C/min
Carrier GasHe, constant flow
Flow Rate:3 mL/min
DetectorFID @ 250 °C
InstrumentAgilent 7890B GC