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Lot-to-Lot Comparison: 1-Hexene on Rxi-LAO

GC_PC1379
PeakstR (min)
1.1-Hexene18.04
2.Hexane18.39
3.2-Ethyl-1-butene19.08
4.cis-3-Hexene19.60
5.trans-2-Hexene19.61
6.cis-3-Methyl-2-pentene20.41
7.cis-2-Hexene20.81
8.trans-3-Methyl-2-pentene21.19
ColumnRxi-LAO, 60 m, 0.25 mm ID, 1.4 µm (cat.# 13876)
Standard/Sample1-Hexene
Conc.: Neat solvent
Injection
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID low pressure drop Precision inlet liner w/wool (cat.# 23309)
Inj. Temp.:250 °C
Split Vent Flow Rate:125 mL/min
Oven
Oven Temp.:35 °C (hold 20 min) to 160 °C at 30 °C/min (hold 20 min)
Carrier GasHe, constant flow
Linear Velocity:23 cm/sec @ 35 °C
DetectorFID @ 300 °C
Make-up Gas Flow Rate:45 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:450 mL/min
Data Rate:20 Hz
InstrumentAgilent 7890B GC
Sample PreparationThe sample was pipetted into a 2 mL vial (cat.# 21142) and capped with a short screw cap (cat.# 24498).