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|Column||Rxi-LAO, 40 m, 0.18 mm ID, 1.0 µm (cat.# 40815)|
|Inj. Vol.:||1 µL split (split ratio 100:1)|
|Liner:||Topaz 4.0 mm ID low pressure drop Precision inlet liner w/wool (cat.# 23309)|
|Inj. Temp.:||250 °C|
|Split Vent Flow Rate:||178 mL/min|
|Oven Temp.:||35 °C (hold 11.85 min) to 160 °C at 50 °C/min (hold 12 min)|
|Carrier Gas||He, constant flow|
|Linear Velocity:||39.19 cm/sec @ 35 °C|
|Detector||FID @ 300 °C|
|Make-up Gas Flow Rate:||45 mL/min|
|Make-up Gas Type:||N2|
|Hydrogen flow:||40 mL/min|
|Air flow:||400 mL/min|
|Data Rate:||20 Hz|
|Instrument||Agilent 7890B GC|
|Sample Preparation||The sample was pipetted into a 2 mL vial (cat.# 21142) and capped with a short screw cap (cat.# 24498).|
|Notes||• Compounds were tentatively identified using a mass spectrometer and method translation. |
• A 208V instrument was used.
• Benzene is not present in the sample, but if it were, it would elute at 12.36 minutes under these conditions.
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