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1-Octene on Rxi-LAO (60 m x 0.25 mm x 1.4 µm)

ColumnRxi-LAO, 60 m, 0.25 mm ID, 1.4 µm (cat.# 13876)
Conc.: Neat solvent
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID low pressure drop Precision liner w/wool (cat.# 23309)
Inj. Temp.:250 °C
Split Vent Flow Rate:125 mL/min
Oven Temp.:35 °C (hold 20 min) to 160 °C at 30 °C/min (hold 20 min)
Carrier GasHe, constant flow
Linear Velocity:23 cm/sec @ 35 °C
DetectorFID @ 300 °C
Make-up Gas Flow Rate:45 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:450 mL/min
Data Rate:20 Hz
InstrumentAgilent 7890B GC
Sample PreparationThe sample was pipetted into a 2 mL vial (cat.# 21142) and capped with a short screw cap (cat.# 24498).
NotesPeaks are tentatively identified.