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1-Octene on Rxi-LAO (40 m x 0.18 mm x 1.0 µm)

ColumnRxi-LAO, 40 m, 0.18 mm ID, 1.0 µm (cat.# 40815)
Conc.: Neat solvent
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID low pressure drop Precision inlet liner w/wool (cat.# 23309)
Inj. Temp.:250 °C
Split Vent Flow Rate:178 mL/min
Oven Temp.:35 °C (hold 11.85 min) to 160 °C at 50 °C/min (hold 12 min)
Carrier GasHe, constant flow
Linear Velocity:39.19 cm/sec @ 35 °C
DetectorFID @ 300 °C
Make-up Gas Flow Rate:45 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:400 mL/min
Data Rate:20 Hz
InstrumentAgilent 7890B GC
Sample PreparationThe sample was pipetted into a 2 mL vial (cat.# 21142) and capped with a short screw cap (cat.# 24498).
Notes• Peaks are tentatively identified.
• A 208V instrument was used.