Opiates (TMS Derivatives) on Rtx-5

GC_PH00233

	Peaks
1.	Meperidine
2.	Alphaprodine
3.	Methadone
4.	Levorphanol (TMS)
5.	Codeine (TMS)

	Peaks
6.	Hydrocodone
7.	Morphine (TMS)
8.	Hydromorphone (TMS)
9.	Oxycodone (TMS)
10.	Oxymorphone (TMS)
11.	Nalorphine (TMS)

Injection
Column	Rtx-5, 30 m, 0.25 mm ID, 0.25 µm (cat.# 10223)
Sample	opiates
Conc.:	2,000 ng/µL
Inj. Vol.:	2.0 µL split (split ratio 50:1)
Inj. Temp.:	250 °C
Oven
Oven Temp.:	200 °C to 325 °C at 7 °C/min
Carrier Gas	He, constant pressure
Linear Velocity:	30 cm/sec @ 200 °C

Detector	MS
Mode:	Scan
Analyzer Type:	Quadrupole
Source Temp.:	300 °C
Ionization Mode:	EI

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