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Peaks | Conc. (wt.%) | |
---|---|---|
1. | Methanol | 0.1 |
2. | Acetaldehyde | 0.2 |
3. | Ethanol | 0.2 |
4. | Isopropanol | 0.1 |
5. | Acetone | 0.01 |
6. | n-Propanol | 0.1 |
Columns | Rtx-BAC1 30 m, 0.32 mm ID, 1.80 µm (cat.# 18003) |
---|---|
and Rtx-BAC2 30 m, 0.32 mm ID, 1.20 µm (cat.# 18002) | |
using two hole ferrule | |
Standard/Sample | 1.0 mL headspace sample of a blood alcohol mix |
Injection | |
Inj. Vol.: | 1,000 µL headspace-syringe split |
Liner: | 2mm ID |
Inj. Temp.: | 200 °C |
Headspace-Syringe | |
Split Vent Flow Rate: | 20 mL/min |
Sample Temp.: | 70 °C |
Sample Equil. Time: | 15 min |
Oven | |
Oven Temp.: | 40 °C |
Carrier Gas | He |
Detector | FID |
---|---|
Instrument | Perkin Elmer HS 40 headspace autosampler |
Notes | Vial pressure: 30 psi Vial pressurization time: 0.15 min. Vial sampling time: 0.01 min. Transfer line: 0.32 mm ID Hydroguard® fused silica tubing Transfer line temp.: 200°C |
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