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Peaks | |
---|---|
1. | Medazepam |
2. | Lorazepam |
3. | Diazepam |
4. | Desmethyldiazepam |
5. | Bromazepam |
6. | Prazepam |
Peaks | |
---|---|
7. | Temazepam |
8. | Flurazepam |
9. | Clobazam |
10. | Flunitrazepam |
11. | Clonazepam |
12. | Alprazolam |
13. | Triazolam |
Column | Rtx-200, 15 m, 0.32 mm ID, 0.25 µm (cat.# 15021) |
---|---|
Standard/Sample | Benzodiazepines |
Conc.: | 15 ng each component |
Injection | |
Inj. Vol.: | 1.0 µL split (split ratio 60:1) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 225 °C to 325 °C at 8 °C/min |
Carrier Gas | He, constant pressure |
Linear Velocity: | 35 cm/sec @ 225 °C |
Detector | FID @ 320 °C |
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Notes | FID sensitivity: 5.12 x 10-10 AFS |