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Peaks | |
---|---|
1. | Methanol |
2. | Ethanol |
3. | Diethyl ether |
4. | Isopropanol |
5. | Methylene chloride |
6. | Acetone |
7. | Methyl tert-butyl ether |
Peaks | |
---|---|
8. | Hexane |
9. | Chloroform |
10. | Ethyl acetate |
11. | Methyl ethyl ketone |
12. | Benzene |
13. | Trichloroethylene |
14. | Toluene |
15. | Methyl isobutyl ketone |
Columns | Rtx-BAC1 30 m, 0.32 mm ID, 1.80 µm (cat.# 18003) |
---|---|
and Rtx-BAC2 30 m, 0.32 mm ID, 1.20 µm (cat.# 18002) | |
Injection | |
Inj. Vol.: | 250 µL headspace-loop |
Headspace-Loop | |
Transfer Line Temp.: | 125 °C |
Sample Temp.: | 70 °C |
Oven | |
Oven Temp.: | 40 °C (hold 4 min) to 120 °C at 10 °C/min |
Carrier Gas | He, constant linear velocity |
Linear Velocity: | 50 cm/sec |
Detector | FID |
---|---|
Notes | Sample loop temp: 125°C |
Acknowledgement | Analyses performed using a Tekmar 7000 Headspace Autosampler on loan courtesy of Tekmar-Dohrmann. |
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