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Peaks | |
---|---|
1. | Methprylon |
2. | Butalbital |
3. | Amobarbital |
4. | Meprobamate |
5. | Glutethimide |
6. | Phenobarbital |
7. | Methaqualone |
8. | Primidone |
Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) |
---|---|
Standard/Sample | 1000μg/mL each |
Diluent: | methanol |
Conc.: | 20 ng each compound on column |
Injection | |
Inj. Vol.: | 1.0 µL split (split ratio 50:1) |
Liner: | Siltek Gooseneck Splitless (4mm) (cat.# 20799-214.5) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 100 °C to 220 °C at 15 °C/min to 330 °C at 10 °C/min (hold 5 min) |
Carrier Gas | He, constant pressure |
Linear Velocity: | 30 cm/sec |
Detector | MS |
---|---|
Mode: | Scan |
Transfer Line Temp.: | 300 °C |
Analyzer Type: | Quadrupole |
Tune Type: | PFTBA |
Ionization Mode: | EI |
Scan Range: | 35-550 amu |
Instrument | HP6890 GC & 5973 MSD |
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