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Acidic/Neutral Drugs Rxi-5ms

GC_PH00815
Peaks
1.Methprylon
2.Butalbital
3.Amobarbital
4.Meprobamate
5.Glutethimide
6.Phenobarbital
7.Methaqualone
8.Primidone
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
Standard/Sample1000μg/mL each
Diluent:methanol
Conc.:20 ng each compound on column
Injection
Inj. Vol.:1.0 µL split (split ratio 50:1)
Liner:Siltek Gooseneck Splitless (4mm) (cat.# 20799-214.5)
Inj. Temp.:250 °C
Oven
Oven Temp.:100 °C to 220 °C at 15 °C/min to 330 °C at 10 °C/min (hold 5 min)
Carrier GasHe, constant pressure
Linear Velocity:30 cm/sec
DetectorMS
Mode:Scan
Transfer Line Temp.:300 °C
Analyzer Type:Quadrupole
Tune Type:PFTBA
Ionization Mode:EI
Scan Range:35-550 amu
InstrumentHP6890 GC & 5973 MSD
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