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Residual Solvents (Class 1) on Stabilwax (G16)

ColumnStabilwax, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10624)
Standard/SampleResidual solvents - class 1 (cat.# 36279)
in 20 mL headspace vial (cat.# 24685)
Diluent:Water
Injection
Inj. Vol.:1.0 µL headspace-syringe split (split ratio 5:1)
Liner:2 mm splitless (cat.# 20712)
Inj. Temp.:140 °C
Headspace-Syringe
Instrument:Overbrook Scientific HT200H
Syringe Temp.:100 °C
Sample Temp.:80 °C
Sample Equil. Time:45 min
Inj. Speed:8
Inj. Dwell:5 sec.
Oven
Oven Temp.:50 °C (hold 20 min) to 165 °C at 6 °C/min (hold 20 min)
Carrier GasHe, constant flow
Flow Rate:2.15 mL/min
Linear Velocity:35.2 cm/sec
DetectorFID @ 250 °C