Residual Solvents (Class 2 - Mixture A) on Stabilwax (G16)

Injection
Column	Stabilwax, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10624)
Standard/Sample	Residual solvents class 2 - mix A (cat.# 36271)
	in 20 mL headspace vial (cat.# 24685)
Diluent:	Water
Inj. Vol.:	1,000 µL headspace-syringe split (split ratio 5:1)
Liner:	2 mm splitless (cat.# 20712)
Inj. Temp.:	140 °C
Headspace-Syringe
Instrument:	Overbrook Scientific HT200H
Syringe Temp.:	100 °C
Sample Temp.:	80 °C
Sample Equil. Time:	45 min
Inj. Speed:	8
Inj. Dwell:	5 sec.
Oven
Oven Temp.:	50 °C (hold 20 min) to 165 °C at 6 °C/min (hold 20 min)
Carrier Gas	He, constant flow
Flow Rate:	2.15 mL/min
Linear Velocity:	35.2 cm/sec

Detector	FID @ 250 °C

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