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Amphetamine and Methamphetamine with salt and free base forms on Rtx-5MS

GC_PH00973
Peaks
1.Amphetamine, free base
2.Amphetamine, salt
3.Methamphetamine, free base
4.Methamphetamine, salt
ColumnRtx®-5MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 12623)
Standard/Sampleamphetamine and methamphetamine
Diluent:methanol
Conc.:100 µg/mL
Injection
Inj. Vol.:1.0 µL split (split ratio 10:1)
Liner:Gooseneck Splitless Siltek (4mm) w/Wool Siltek Liner
Inj. Temp.:250 °C
Oven
Oven Temp.:70 °C to 250 °C at 15 °C/min (hold 5 min)
Carrier GasH2, constant flow
Flow Rate:1 mL/min
DetectorFID @ 300 °C
NotesGooseneck Splitless (4mm) w/Wool Siltek Liner obsolete, recommend catalog number 20798