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Peaks | |
---|---|
12. | di-Isopropyl sulfate (DPS) |
13. | di-n-Propyl sulfate (DNS) |
14. | Dibutyl sulfate (DBS) |
15. | Methylbenzene sulfonate (MBS) |
16. | Ethylbenzene sulfonate (EBS) |
17. | Methyl toluenesulfonate (MTS) |
18. | Ethyl toluenesulfonate (ETS) |
19. | n-Butyl benzenesulfonate (nBBS) |
20. | n-Propyl toluenesulfonate (nPTS) |
21. | Isopropyl toluenesulfonate (iPTS) |
22. | n-Butyl toluenesulfonate (nBTS) |
Column | Rtx-200, 30 m, 0.25 mm ID, 1.0 µm (cat.# 15053) |
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Standard/Sample | |
Diluent: | 90:10 acetonitrile:water |
Conc.: | 100 µg/mL |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 10:1) |
Liner: | 4mm Gooseneck Splitless w/Wool (cat.# 22405) |
Inj. Temp.: | 220 °C |
Oven | |
Oven Temp.: | 40 °C (hold 8.3 min) to 70 °C at 70 °C/min to 115 °C at 40 °C/min to 250 °C at 30 °C/min to 300 °C at 15 °C/min (hold 3 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 1 mL/min |
Detector | MS |
---|---|
Mode: | Scan |
Transfer Line Temp.: | 280 °C |
Ionization Mode: | EI |
Scan Range: | 20-250 amu |
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