Residual Solvents Rxi-624Sil MS

Injection
Column	Rxi-624Sil MS, 30 m, 0.32 mm ID, 1.80 µm (cat.# 13870)
Standard/Sample	Residual Solvents Class 2 - Mix B (cat.# 36280)
Conc.:	83 µL in 6 mL water in a 20mL headspace vial. (Conc. not consistent with USP <467> methodology.)
Inj. Vol.:	1000 µL headspace-syringe split (split ratio 3:1)
Liner:	1mm Split (cat.# 20972)
Inj. Temp.:	140 °C
Oven
Oven Temp.:	40 °C (hold 20 min) to 240 °C at 10 °C/min (hold 20 min)
Carrier Gas	He, constant flow
Flow Rate:	2.2 mL/min

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