Residual Solvents Class 2 - Mix A (2013 Rev) on Stabilwax (G16)

Injection
Column	Stabilwax, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10624)
Standard/Sample	Residual Solvents Class 2 - Mix A (2013 Rev) (cat.# 36012)
Diluent:	Water
Conc.:	Per USP <467> method
Inj. Vol.:	1,000 µL headspace-loop split (split ratio 50:1)
Liner:	Premium 1.0 mm ID straight inlet liner (cat.# 23333.1)
Headspace-Loop
Inj. Port Temp.:	140 °C
Instrument:	Tekmar HT3
Inj. Time:	1.0 min
Transfer Line Temp.:	105 °C
Valve Oven Temp.:	105 °C
Needle Temp.:	80 °C
Standby flow rate:	50 mL/min
Sample Temp.:	80 °C
Platen temp equil. time:	1.0 min
Sample Equil. Time:	45 min
Mixer time:	5.0 min
Mixing level:	5
Mixer stabilize time:	0.50 min
Vial Pressure:	20 psi
Pressurize Time:	5.0 min
Pressure Equilibration Time:	0.20 min
Loop Pressure:	10 psi
Loop Fill Time:	2.0 min
Oven
Oven Temp.:	50 °C (hold 20 min) to 165 °C at 6 °C/min (hold 20 min)
Carrier Gas	He, constant flow
Flow Rate:	2.2 mL/min
Linear Velocity:	36 cm/sec @ 50 °C

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