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Peaks | Ion | Cone V | |
---|---|---|---|
1. | Aldicarb sulfone | 223.3 | 25V |
2. | Aldicarb sulfoxide | 207.3 | 18V |
3. | Oxamyl | 237.2* | 10V |
4. | Methomyl | 163.2 | 15V |
5. | 3-Hydroxycarbofuran | 238.3 | 15V |
6. | Aldicarb | 191.2 | 8V |
7. | Propoxur | 210.2 | 18V |
8. | Carbofuran | 222.3 | 22V |
9. | Carbaryl | 202.2 | 18V |
10. | Methiocarb | 226.3 | 19V |
Column | Ultra Carbamate (cat.# 9177315) | ||||||||
---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 4.6 mm ID | ||||||||
Particle Size: | 3 µm | ||||||||
Pore Size: | 100 Å | ||||||||
Standard/Sample | |||||||||
Conc.: | 100 µg/mL each component | ||||||||
Inj. Vol.: | 10 µL | ||||||||
Mobile Phase | |||||||||
A: | 90% water:10% methanol with 10mM ammonium formate | ||||||||
B: | 90% acetonitrile:10% methanol with 10mM ammonium formate | ||||||||
| |||||||||
Flow: | 1.0 mL/min |
Detector | UV/Vis @ 220 nm |
---|---|
Notes | Flow: (approx. 0.75mL/min. to UV detector, 0.25mL/min. to MSD) MSD Conditions: Detector: Micromass ZMD Mode: ESI+ Capillary V: 3.50 Extractor: 4.0 Ion energy: 0.4 Multiplier: 650 Source temp: 100°C Desolv. temp: 250°C Gas flow: 490 L/hr. |
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