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Peaks | tR (min) | SIM | |
---|---|---|---|
1. | Bromazepam | 1.23 | 317.95 |
2. | Flurazepam | 1.36 | 388.10 |
3. | Oxazepam | 2.05 | 287.05 |
4. | Nitrazepam | 2.16 | 282.05 |
5. | Lorazepam | 2.20 | 321.00 |
6. | Alprazolam | 2.55 | 316.00 |
Peaks | tR (min) | SIM | |
---|---|---|---|
7. | Clonazepam | 2.61 | 309.05 |
8. | Triazolam | 2.71 | 343.05 |
9. | Temazepam | 3.02 | 301.05 |
10. | Flunitrazepam | 3.25 | 314.05 |
11. | Clobazam | 3.28 | 301.05 |
12. | Diazepam | 3.54 | 285.05 |
Column | Raptor Biphenyl (cat.# 9309A12) | ||||||||||||||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||||||||||||||
Temp.: | 40 °C | ||||||||||||||||||||||||||||||||
Standard/Sample | |||||||||||||||||||||||||||||||||
Diluent: | Water:acetonitrile (70:30) | ||||||||||||||||||||||||||||||||
Conc.: | 5 µg/mL | ||||||||||||||||||||||||||||||||
Inj. Vol.: | 1 µL | ||||||||||||||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||||||||||||||
A: | 2 mM Ammonium formate + 0.2% formic acid in water | ||||||||||||||||||||||||||||||||
B: | 0.2% Formic acid in acetonitrile | ||||||||||||||||||||||||||||||||
|
Detector | Shimadzu LCMS-2010EV |
---|---|
Acquisition Type: | Scan/SIM |
Probe Voltage: | 1.5 kV |
Nebulizing Gas Flow: | 1.5 L/min |
Drying Gas Pressure: | 0.1 MPa |
CDL Temp.: | 300 °C |
Heat Block: | 300 °C |
Interface: | ESI+ |
Instrument | Shimadzu UFLCXR |
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