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Peaks | tR (min) | Precursor Ion | Product Ion | Product Ion | |
---|---|---|---|---|---|
1. | 2-Oxo-3-hydroxy-LSD | 1.21 | 356.3 | 237.0 | 222.0 |
2. | Dextrorphan | 1.31 | 258.2 | 157.0 | 201.2 |
3. | LSD | 1.46 | 324.3 | 223.1 | 208.0 |
4. | Dextromethorphan | 1.57 | 272.2 | 215.1 | 170.9 |
5. | PCP | 1.60 | 244.2 | 86.1 | 159.1 |
6. | 25I-NBOMe | 1.80 | 428.1 | 121.2 | 91.1 |
Column | Raptor Biphenyl (cat.# 9309A12) | ||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||
Particle Size: | 2.7 µm | ||||||||||||||||||||
Guard Column: | Raptor Biphenyl EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9309A0252) | ||||||||||||||||||||
Temp.: | 50 °C | ||||||||||||||||||||
Standard/Sample | |||||||||||||||||||||
Diluent: | Water | ||||||||||||||||||||
Conc.: | 10 ng/mL | ||||||||||||||||||||
Inj. Vol.: | 5 µL | ||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||
A: | Water + 0.1% formic acid | ||||||||||||||||||||
B: | Acetonitrile + 0.1% formic acid | ||||||||||||||||||||
|
Detector | MS/MS |
---|---|
Ion Mode: | ESI+ |
Mode: | MRM |
Instrument | UHPLC |
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